UK Anti-Doping Annual Report and Accounts 2015/16 / United Kingdom Anti-Doping (UKAD). - London : UKAD, 2016
- Print ISBN 9781474131599
- Web ISBN 9781474131605
UK Anti-Doping Annual Report and Accounts 2015/16 / United Kingdom Anti-Doping (UKAD). - London : UKAD, 2016
UK Anti-Doping Annual Report and Accounts 2016/17 / United Kingdom Anti-Doping (UKAD). - London : UKAD, 2017
UK Anti-Doping Annual Report and Accounts 2017/18 / United Kingdom Anti-Doping (UKAD). - London : UKAD, 2018
UK Anti-Doping Annual Report and Accounts 2018/19 / United Kingdom Anti-Doping (UKAD). - London : UKAD, 2019
UK Anti-Doping Annual Report and Accounts 2019/20 / United Kingdom Anti-Doping (UKAD). - London : UKAD, 2021
UK Anti-Doping Annual Report and Accounts 2020/21 / United Kingdom Anti-Doping (UKAD). - London : UKAD, 2021
UK Anti-Doping Annual Report and Accounts 2021/22 / United Kingdom Anti-Doping (UKAD). - London : UKAD, 2022
Ultra trace detection of a wide range of anabolic steroids in meat by gas chromatography coupled to mass spectrometry / P. Marchand, B. le Bizec, C. Gade, F. Monteau, F. André
Abstract
The control on use of anabolic agents in meat producing animals is generally based on urine, faeces or hair analysis. This exercise, which is usually performed in slaughterhouses or on farms, is not relevant to imported carcasses or retail meat. A single sensitive method for a wide range of anabolic steroids was developed. After extraction of the lyophilised meat, enzymatic hydrolysis was used for deconjugation. Solid-phase extraction on a polymeric stationary phase was performed prior to hydrolysis of ester residues under alkaline conditions. Liquid-liquid partitioning was used to separate the analytes into two main categories: phenol containing molecules, such as phenolic steroids, resorcylic acid lactones and stilbenes, and delta4-3-one containing molecules, such as most androgens and progestagens. Solid-phase extraction on silica columns was performed before applying a specific derivatisation for each compound sub-group. The combination of high-resolution chromatography with a quadrupole mass spectrometer permitted detection of 23 steroids in the 5-100 ng/kg range. Ion chromatograms for residue positive samples are shown and discussed.
Onzeker over doping? (Dutch title)
This leaflet gives some basic information on doping and doping issues like: what is doping, what substances are prohibited, why do people cheat, why is there such a fuss made about doping? THe leaflet is made for adolescent athletes.
Undeclared Doping Substances are Highly Prevalent in Commercial Sports Nutrition Supplements / Erik Duiven, Luc J.C. van Loon, Laila Spruijt, Willem Koert, Olivier M. de Hon. -
(Journal of Sports Science and Medicine 20 (2021); p. 328-338)
ABSTRACT
Sports nutrition supplements have previously been reported to contain undeclared doping substances. The use of such supplements can lead to general health risks and may give rise to unintentional doping violations in elite sports. To assess the prevalence of doping substances in a range of high-risk sports nutrition supplements available from Dutch web shops. A total of 66 sports nutrition supplements - identified as potentially high-risk products claiming to modulate hormone regulation, stimulate muscle mass gain, increase fat loss, and/or boost energy - were selected from 21 different brands and purchased from 17 web shops. All products were analyzed for doping substances by the UK life sciences testing company LGC, formerly known as the Laboratory of the Government Chemist, using an extended version of their ISO17025 accredited nutritional supplement screen. A total of 25 out of the 66 products (38%) contained undeclared doping substances, which included high levels of the stimulants oxilofrine, β-methylphenethylamine (BMPEA) and N,β-dimethylphenethylamine (NBDMPEA), the stimulant 4-methylhexan-2-amine (methylhexaneamine, 1,3-dimethylamylamine, DMAA), the anabolic steroids boldione (1,4-androstadiene-3,17-dione) and 5-androstene-3β,17α-diol (17α-AED), the beta-2 agonist higenamine and the beta-blocker bisoprolol. Based upon the recommended dose and the potential variability of analyte concentration, the ingestion of some products identified within this study could pose a significant risk of unintentional doping violations. In addition to inadvertent doping risks, the prescribed use of 3 products (4.5%) could likely impose general health risks.